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Use filter tips, double gloves, bleach waste, GMO desinfectant, desinfect all plastic material before disposal.
Day 1 - HEK replate
- Re-seed HEK cells to obtain 10-20% confluence (ideally early in the morning)
- After HEK adhesion (late afternoon) proceed with transfection using either Fugene or Lipofectamine 3000
Day 1A - Transfection by Fugene
- Confirm plasmids concentration and prepare the mix of packaging plasmids
- plasmid #9: 1750ng
- plasmid #10: 3240ng
- plasmid of interest: 5000ng.
- Equlibrate Optimem to RT
- Vortex and spin down Fugene
- Dilute plasmid mix in 1mL Optimem, vortex, spin down
- Add 30uL of Fugene, mix by inverstion incubate 5-15minutes at RT
- Apply dropwise to 10cm dish
- Incubate overnight
Day 1B - Transfection by Lipofectamine
- Confirm plasmids concentration and prepare the mix of packaging plasmids
- plasmid #9: 1750ng
- plasmid #10: 3240ng
- plasmid of interest: 5000ng.
- Equlibrate Optimem and Lipofectamine components to RT
- Vortex and spin down components
- Solution A: Dilute 35uL of Lipofectamine in 875uL of Optimem, vortex, spin
- Solution B: Dilute 20uL of P3000 from Lipofect kit in 875uL of Optimem, add your plasmids, mix by pipetting
- Mix A and B, incubate 10-15 min at RT
- Apply dropwise to 10cm dish
- Incubate overnight
Day 2 - Exchange media
Change media to 10 %KOSR in DMEM high Glucose (15mL)
Day 3-5 collect media with viral particles
- Collect media
- Put fresh 10 %KOSR in DMEM high Glucose (15mL)
- SPin down debris in collected media using 3000g for 10min
- Filter using 0.45um filter
- Store at 4°C
Day 5 Concentrate particles
NOTE: may not be needed for well transducable cells such as HEK, Cal51
- Use Vivaspin Concentrator spin columns
- Centrifuge particles at 3000g at 4°C for 15 min
- Check if they are concentrated enough if not repeat (I concentrate 20-40x for CMs)
- Store concentrated at 4°C for up to 1 month
Transduction test
- Seed your cells in 24 well
- Test ratio of viral particles / media in range 4to1 to 0.25to1
- Check after 24hours what concnetration works best
Transduction
- Prepare culture media with Polybrene 5-10ug/mL stock 10mg/mL 7.5ug/mL works good(VV)
- Add particles dropwise to wells
- Check after 24 hours
Plasmids
- Packaging #9: Addgene #12259; Stored in Sofia’s freezer top right drawer
- Packaging #10: Addgene#12260; Stored in Sofia’s freezer top right drawer
- YAP1-OE #124: Addgene#74942; in Vladmir’s green box in IPSc
Material
Transfection reagents (IPSCs fridge)
- Lipofectamine 3000 Thermofisher Web Link; CatNo: L3000-15; Current Lot:2153940
- Fugene HD transfection reagent; Promega Web Link ; CatNo: E2311; Lot:000064305J
- Optimem Thermofisher web link
Collection and concentration
- 50mL syringe
- 0.45um filters
- Concentration columns Vivaspin 20PES, 100kDa; in western-blot cabinet bottom shelf, the one with blue tops
Transduction
- Polybrene Sigma Aldrich: 10mg/mL; in cell culture freezer, upper right mbd drawer in 50mL falcon (20F1 B2)